Recent content by lamejane

  1. lamejane

    A Why Do Voids Form at the Thin-Film Substrate Interface After Annealing?

    Thank you for your reply. Using the Hot plate was only for test purposes. For the the long term i would move to a RTA tool as you suggested. Lets say the process is carried out in an RTA und N2 atmosphere , what effect does a longer annealing tme ( ~ 60 min ) have on the metal layers ? Why is...
  2. lamejane

    A Why Do Voids Form at the Thin-Film Substrate Interface After Annealing?

    Hello to all the experts out there!: ) I have encountered a problem on my samples after Post deposition annealing [ Please refer to the crossectional SEM picture - B below]. Sample description : Thinfilm metal stack [ Pd/Ti/Pd/Au] deposited onto GaAs substrate using PVD Post deposition...
  3. lamejane

    PVD Vaccum Chamber -- How to clean up after Water leakage?

    Thank you, This suggestion along with heating the chamber walls with a hot blowdryer (industry grade) prior to chamber evacuation helped. We have no Leaks.
  4. lamejane

    PVD Vaccum Chamber -- How to clean up after Water leakage?

    the root cause is unkown but we suspect that the seals were faulty.
  5. lamejane

    PVD Vaccum Chamber -- How to clean up after Water leakage?

    Hello all , our PVD chamber experienced a water leakage from the cruible revoler area and unfortunately we are no longer able to achieve a stable Base pressure ( ~10e-6 mbar) We do not have the option of a bake out. Is there any other way to get rid of water in the chamber ? Ofcourse the water...
  6. lamejane

    EPVD: Effect of changing the Thin-film Metal deposition Rate

    Hello Material experts out there ! I would like to test a reduced deposition rate for Ni ( 0.3 nm/sec reduced to 0.1 nm/sec) to avoid metal splashes and stabilize the process. This would for sure increase the deposition process time but I'm not quite sure of the Microscopic effects of such a...
  7. lamejane

    E-PVD Vacuum chamber cleaning maintenance and Care

    Not really, they don't really suggest what to use in order to clean but only give a time period of when to perform a cleaning and maintainence
  8. lamejane

    E-PVD Vacuum chamber cleaning maintenance and Care

    Hello PVD experts out there ! I have question on general e-PVD Vacuum chamber cleaning maintenance and Care as shown in the pictures below, Thin film material (mostly Metals) is being deposited on a daily basis onto the hardware parts present in our e-PVD vacuum chamber ( such as the quartz...
  9. lamejane

    E-beam Physical Vapour deposition

    Thank you for the reply!, i shall give a shot with Al2O3 or WC liners for Ni and Pt.
  10. lamejane

    E-beam Physical Vapour deposition

    Hello, a) Yes, the rise time is set to 2 min and soak time is set to1 min [ Ni and Pt]. Both have a point beam spot instead of x-y wobbling. the spot size can be changed if required. The spot type can also be changed to spiral, wobble and X- scan. b) Yes the chamber is Opened after each...
  11. lamejane

    E-beam Physical Vapour deposition

    Hope we have some PVD specialists in the house :) we have a pfeiffer e-beam PVD in the lab which i use to deposit Ni and Pt thin films ( around 100nm each) on Si wafers. I have always had the problem of "Ni splashes" while heating the target ( with the e beam) which leads to a process stop (...
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